(R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide

Base Information

• Chemical Name: (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide
• CAS No.: 1259080-07-3
• Molecular Formula: C₂₀H₂₄BrNOS
• Molecular Weight: 406.387

Synonyms:(R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide

Chemical Property of (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide

Chemical Property:

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Technology Process of (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide

There total 3 articles about (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(R)-N-benzylidene-2-methylpropane-2-sulfinamide (196929-85-8) + 1-(4-bromophenyl)-1-propen-3-yl bromide (96090-12-9,124854-99-5) → (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide (1259080-07-3)

Guidance literature:

With lithium chloride; zinc; In N,N-dimethyl-formamide; at 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1039/c0cc03230a

Reference yield:

(R)-N-benzylidene-2-methylpropane-2-sulfinamide (196929-85-8) + 1-(4-bromophenyl)-1-propen-3-yl bromide (96090-12-9,124854-99-5) → C20H24BrNOS (1259080-71-1) + (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide (1259080-07-3)

Guidance literature:

With lithium chloride; zinc; In tetrahydrofuran; at 20 ℃; optical yield given as %ee; Inert atmosphere;

DOI:10.1039/c0cc03230a

Reference yield:

(R)-N-benzylidene-2-methylpropane-2-sulfinamide (196929-85-8) + 1-(4-bromophenyl)-1-propen-3-yl bromide (96090-12-9,124854-99-5) → C20H24BrNOS (1259080-71-1) + (R)-N-((1R,2R)-2-(4-bromophenyl)-1-phenylbut-3-enyl)-2-methylpropane-2-sulfinamide (1259080-07-3) + C20H24BrNOS

Guidance literature:

With zinc; In tetrahydrofuran; at 20 ℃; optical yield given as %ee;

DOI:10.1039/c0cc03230a

upstream raw materials:

(R)-N-benzylidene-2-methylpropane-2-sulfinamide

1-(4-bromophenyl)-1-propen-3-yl bromide

Downstream raw materials:

C₁₆H₁₆BrN

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