D-XYLONIC ACID, CALCIUM SALT, HYDRATE

Base Information

• Chemical Name: D-XYLONIC ACID, CALCIUM SALT, HYDRATE
• CAS No.: 72656-08-7
• Molecular Formula: 2C₅H₉O₆*Ca
• Molecular Weight: 370.324
• Mol file: 72656-08-7.mol

Synonyms:D-XYLONIC ACID, CALCIUM SALT, HYDRATE;CALCIUM D-XYLONATE HYDRATE

Chemical Property of D-XYLONIC ACID, CALCIUM SALT, HYDRATE

Chemical Property:

• Melting Point: 118 °C
• PSA: 232.90000
• LogP: -5.99080
• Storage Temp.: -20°C Freezer
• Solubility.: Water (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

D-Xylonic Acid, Calcium Salt, Hydrate ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Uses: D-Xylonic Acid Calcium Salt Hydrate is a compound useful in organic synthesis.

Technology Process of D-XYLONIC ACID, CALCIUM SALT, HYDRATE

There total 2 articles about D-XYLONIC ACID, CALCIUM SALT, HYDRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

potassium 4-keto-D-arabonate (15770-22-6) → D-arabinoic acid calcium salt (5346-83-8,7546-24-9,18905-33-4,22373-09-7,56512-56-2,62102-50-5,72656-08-7,74440-84-9,76386-31-7,123249-13-8,123277-10-1,133480-82-7,133480-83-8)

Guidance literature:

With calcium acetate; In water; a.) reflux, 1 h, b.) 0 to 5 deg C, 6 h;

DOI:10.1016/0008-6215(91)80010-K

Reference yield:

D-arabinoic acid calcium salt (5346-83-8,7546-24-9,18905-33-4,22373-09-7,56512-56-2,62102-50-5,72656-08-7,74440-84-9,76386-31-7,123249-13-8,123277-10-1,133480-82-7,133480-83-8) → calcium D-ribonate (5346-83-8,7546-24-9,18905-33-4,22373-09-7,56512-56-2,62102-50-5,72656-08-7,74440-84-9,76386-31-7,123249-13-8,123277-10-1,133480-82-7,133480-83-8)

Guidance literature:

With calcium hydroxide; In water; at 137 ℃; for 5h;

DOI:10.1016/0008-6215(91)80010-K

Reference yield:

calcium D-ribonate (5346-83-8,7546-24-9,18905-33-4,22373-09-7,56512-56-2,62102-50-5,72656-08-7,74440-84-9,76386-31-7,123249-13-8,123277-10-1,133480-82-7,133480-83-8) → (4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-dihydro-furan-2-one (2782-09-4,3327-63-7,5336-08-3,13280-76-7,15384-34-6,15384-37-9,17676-01-6,18423-66-0,51532-86-6,68035-75-6,104196-15-8,133908-85-7) + D-Ribono-1,4-lactone (5336-08-3)

Guidance literature:

With sulfuric acid; In water; Yield given;

DOI:10.1016/0008-6215(91)80010-K

upstream raw materials:

potassium 4-keto-D-arabonate

D-arabinoic acid calcium salt

Downstream raw materials:

calcium D-ribonate

(4S,5R)-3,4-Dihydroxy-5-hydroxymethyl-dihydro-furan-2-one

D-Ribono-1,4-lactone