carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate

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Chemical Name:carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate
CAS No.:130390-28-2
Molecular Formula:C₃₅H₅₈O₅P₂RhSi₂*F₆P
Molecular Weight:924.831
Hs Code.:

Synonyms:carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate

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Chemical Property of carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate

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Technology Process of carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate

There total 1 articles about carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 130390-24-8
tricarbonyl-trans-bis{(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane}rhodium(I)-hexafluorophosphate

: 130390-28-2
carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate

Guidance literature:: In dichloromethane; byproducts: CO; bubbling of Ar (20°C, 30 min) through the soln.;; NMR, IR, elem. anal; MS;;
DOI:10.1016/0022-328X(90)85069-B

Reference yield: 92.0%

: 130390-28-2
carbonyl-trans-bis(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-P;O',P'}rhodium(I)-hexafluorophosphate

: a-acetyl-b-iodo-fc,ed-bis{(1,4-dioxanyl-2-methyl)phenyl(3-trimethylsilylpropyl)phosphane-O,P}rhodium(III)-hexafluorophosphate

Guidance literature:: With methyl iodide; In dichloromethane; under Ar; stirring at room temperature, after 5h removal of volatile compounds in vacuum;; washing with pentane, IR, NMR, elem. anal; MS;
DOI:10.1016/0022-328X(90)85069-B