C₁₆H₁₆O₄

Base Information

• Chemical Name: C₁₆H₁₆O₄
• CAS No.: 1018987-81-9
• Molecular Formula: C₁₆H₁₆O₄
• Molecular Weight: 272.301
• Mol file: 1018987-81-9.mol

Synonyms:C₁₆H₁₆O₄

Chemical Property of C₁₆H₁₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₆O₄

There total 3 articles about C₁₆H₁₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

terephthalaldehyde, (623-27-8) + 2-methylphenyl aldehyde (529-20-4) → C16H16O4 (1018987-81-9) + 4-(6-O-tolyl[1,2,4,5]tetroxan-3-yl)benzaldehyde (1312772-69-2)

Guidance literature:

2-methylphenyl aldehyde; With MeReO₃; dihydrogen peroxide; In 2,2,2-trifluoroethanol; water; at 20 ℃; for 2h;

terephthalaldehyde,; With tetrafluoroboric acid; In diethyl ether; 2,2,2-trifluoroethanol; water; at 20 ℃; for 1h;

DOI:10.1016/j.ejmech.2011.04.002

Reference yield: 19.0%

2-methylphenyl aldehyde (529-20-4) → C16H16O4 (1018987-81-9)

Guidance literature:

2-methylphenyl aldehyde; With dihydrogen peroxide; methyltrioxorhenium(VII); In 2,2,2-trifluoroethanol; at 20 ℃; for 2h;

2-methylphenyl aldehyde; With tetrafluoroboric acid; In diethyl ether; 2,2,2-trifluoroethanol; at 20 ℃; for 1h; Further stages.;

DOI:10.1016/j.bmcl.2007.12.069

Reference yield:

1-(dihydroperoxymethyl)-2-methylbenzene + 2-methylphenyl aldehyde (529-20-4) → C16H16O4 (1018987-81-9)

Guidance literature:

With tetrafluoroboric acid diethyl ether; In acetonitrile; at 20 ℃;

DOI:10.1016/j.bmcl.2009.01.103

upstream raw materials:

2-methylphenyl aldehyde

terephthalaldehyde,