Technology Process of methyl 3,4-di-O-benzyl-6-O-trityl-α-D-glucopyranoside
There total 5 articles about methyl 3,4-di-O-benzyl-6-O-trityl-α-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 20 ℃;
for 2.5h;
Inert atmosphere;
DOI:10.1002/ejoc.200900310
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 3 h / 90 °C
2.1: tetra-(n-butyl)ammonium iodide; di(n-butyl)tin oxide / acetonitrile / 16 h / 82 °C / Soxhlet apparatus; Molecular sieve
3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0 °C
3.2: 0 - 20 °C
4.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2.5 h / 20 °C / Inert atmosphere
With
pyridine; water; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.200900310
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 3 h / 90 °C
2.1: tetra-(n-butyl)ammonium iodide; di(n-butyl)tin oxide / acetonitrile / 16 h / 82 °C / Soxhlet apparatus; Molecular sieve
3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0 °C
3.2: 0 - 20 °C
4.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2.5 h / 20 °C / Inert atmosphere
With
pyridine; water; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.200900310
