N-Benzoyl-zimtsaeure-amid

Base Information

• Chemical Name: N-Benzoyl-zimtsaeure-amid
• CAS No.: 893-40-3
• Molecular Formula: C₁₆H₁₃NO₂
• Molecular Weight: 251.285
• Mol file: 893-40-3.mol

Synonyms:N-Benzoyl-zimtsaeure-amid

Chemical Property of N-Benzoyl-zimtsaeure-amid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Benzoyl-zimtsaeure-amid

There total 2 articles about N-Benzoyl-zimtsaeure-amid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

cinnamamide (621-79-4) + benzyl alcohol (100-51-6,185532-71-2) → N-Benzoyl-zimtsaeure-amid (893-40-3)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; 9-azanoradamantane N-oxyl; potassium tert-butylate; oxygen; copper(l) chloride; In tetrahydrofuran; at 23 ℃; for 24h; Molecular sieve;

DOI:10.1039/c8sc01410h

Reference yield:

→ N-Benzoyl-zimtsaeure-amid (893-40-3)

Guidance literature:

Benzamid, Zimtsaeure-chlorid, Bl., Δ;

Reference yield: 91.0%

tributylphosphine (998-40-3) + N-Benzoyl-zimtsaeure-amid (893-40-3) → (3-benzamido-3-oxo-1-phenylpropyl)tributylphosphonium chloride

Guidance literature:

With hydrogenchloride; benzoyl chloride; In dichloromethane; water; at 30 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.9b03116

upstream raw materials:

cinnamamide

benzyl alcohol

Downstream raw materials:

C₂₃H₂₄N₂O₃

C₂₃H₂₂N₂O₃

N-benzoylbenzamide

tribenzamide