2-(4-Phenoxyphenoxy)ethanethiol

Base Information

Chemical Name:2-(4-Phenoxyphenoxy)ethanethiol
CAS No.:87545-50-4
Molecular Formula:C₁₄H₁₄O₂S
Molecular Weight:246.33
Hs Code.:
DSSTox Substance ID:DTXSID601304778

Synonyms:2-(4-phenoxyphenoxy)ethanethiol;SCHEMBL11028328;DTXSID601304778;AKOS017554279;87545-50-4

Suppliers and Price of 2-(4-Phenoxyphenoxy)ethanethiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(4-Phenoxyphenoxy)ethanethiol

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:246.07145086
Heavy Atom Count:17
Complexity:196

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)OC2=CC=C(C=C2)OCCS

Technology Process of 2-(4-Phenoxyphenoxy)ethanethiol

There total 5 articles about 2-(4-Phenoxyphenoxy)ethanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: S-(2-(4-phenoxyphenoxy)ethyl) ethanethioate

: 87545-50-4
2-(4-phenoxyphenoxy)ethanethiol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.1002/cmdc.201600505

Reference yield:

: 88356-00-7
(4-phenoxyphenoxyethyl)-4-toluenesulfonate

: 87545-50-4
2-(4-phenoxyphenoxy)ethanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / dimethylformamide / 3 h / 100 °C

2: 1.) NaOCH₃, 2.) gl. AcOH, Zn / 1.) MeOH, RT, 2 h, 2.) reflux, 1 h

With sodium methylate; acetic acid; zinc; In N,N-dimethyl-formamide;
DOI:10.1021/jm970860z

Reference yield:

: 63066-74-0
2-(4-phenoxyphenoxy)-ethanol

: 87545-50-4
2-(4-phenoxyphenoxy)ethanethiol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyridine, 2.) aq. HCl / 1.) RT, 4 h, 2.) RT, 1 h

2: 73 percent / dimethylformamide / 3 h / 100 °C

3: 1.) NaOCH₃, 2.) gl. AcOH, Zn / 1.) MeOH, RT, 2 h, 2.) reflux, 1 h

With pyridine; hydrogenchloride; sodium methylate; acetic acid; zinc; In N,N-dimethyl-formamide;
DOI:10.1021/jm970860z