Technology Process of C47H63N8O19S(1-)*Na(1+)
There total 7 articles about C47H63N8O19S(1-)*Na(1+) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.116
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylsilane; trifluoroacetic acid / dichloromethane
2: hydrogen; palladium on activated charcoal / water
3: sodium hydroxide / water; 1,4-dioxane
4: lithium hydroxide / water; N,N-dimethyl-formamide
5: methanesulfonyl chloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
With
triethylsilane; palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; lithium hydroxide;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.116
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen; palladium on activated charcoal / water
2: sodium hydroxide / water; 1,4-dioxane
3: lithium hydroxide / water; N,N-dimethyl-formamide
4: methanesulfonyl chloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
With
palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; lithium hydroxide;
In
1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.116