(3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

Base Information

Chemical Name:(3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone
CAS No.:1380547-98-7
Molecular Formula:C₃₃H₂₇NO₂
Molecular Weight:469.583
Hs Code.:

Synonyms:(3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

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Chemical Property of (3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

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Technology Process of (3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

There total 6 articles about (3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92-69-3
4-Phenylphenol

: 1380547-65-8
(3-(hydroxymethyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

: 1380547-98-7
(3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine;
DOI:10.1016/j.bmcl.2012.04.023

Reference yield:

: 879-18-5
naphthalene-1-carbonic acid chloride

: 1380547-98-7
(3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane

2: lithium borohydride / methanol

3: di-isopropyl azodicarboxylate; triphenylphosphine

With lithium borohydride; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In methanol; dichloromethane; 3: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.04.023

Reference yield:

: 1380547-78-3
C₂₃H₂₁NO₃

: 1380547-98-7
(3-(([1,1'-biphenyl]-4-yloxy)methyl)-3,4-dihydroisoquinolin-2(1H)-yl)(naphthalen-1-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: lithium borohydride / methanol

2: di-isopropyl azodicarboxylate; triphenylphosphine

With lithium borohydride; di-isopropyl azodicarboxylate; triphenylphosphine; In methanol; 2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.04.023