ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

Base Information

Chemical Name:ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate
CAS No.:1263870-17-2
Molecular Formula:C₂₄H₃₁NO₅
Molecular Weight:413.514
Hs Code.:

Synonyms:ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

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Chemical Property of ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

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Technology Process of ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

There total 4 articles about ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 76041-06-0
ethyl 3-[(2-ethoxycarbonyl)ethylamino]-2-phenylpropionate

: 2746-25-0
p-Methoxybenzyl bromide

: 1263870-17-2
ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

Guidance literature:: With potassium carbonate; In acetone; for 3h; Reflux;

Reference yield:

: 140-29-4
phenylacetonitrile

: 1263870-17-2
ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / -10 °C

1.2: -10 - 40 °C

2.1: hydrogen; trifluoroacetic acid / palladium 10% on activated carbon / methanol / 3 h / 20 °C / 3677.86 Torr

3.1: ethanol / 18 h / 20 °C

4.1: potassium carbonate / acetone / 3 h / Reflux

With hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; acetone;

Reference yield:

: 4553-07-5
ethyl phenylcyanoacetate

: 1263870-17-2
ethyl 3-((3-ethoxy-3-oxopropyl)(4-methoxybenzyl)amino)-2-phenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; trifluoroacetic acid / palladium 10% on activated carbon / methanol / 3 h / 20 °C / 3677.86 Torr

2: ethanol / 18 h / 20 °C

3: potassium carbonate / acetone / 3 h / Reflux

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium 10% on activated carbon; In methanol; ethanol; acetone;