9-O-Benzoylheliotridine

Base Information

Chemical Name:9-O-Benzoylheliotridine
CAS No.:126191-51-3
Molecular Formula:C₁₅H₁₇NO₃
Molecular Weight:259.305
Hs Code.:

Synonyms:9-O-Benzoylheliotridine

Suppliers and Price of 9-O-Benzoylheliotridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-O-Benzoylheliotridine

Chemical Property:

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Technology Process of 9-O-Benzoylheliotridine

There total 1 articles about 9-O-Benzoylheliotridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 65-85-0,8013-63-6
benzoic acid

: 520-63-8
(+)-heliotridine

: 126191-51-3
9-O-Benzoylheliotridine

Guidance literature:: With 1,1'-carbonyldiimidazole; In tetrahydrofuran; for 20h; Ambient temperature;
DOI:10.1021/jo00297a081

Reference yield: 62.0%

: 126191-51-3
9-O-Benzoylheliotridine

: 1005-56-7
phenylcarbonochloridothioate

: 126191-54-6
7-O-(Phenoxythiocarbonyl)-9-O-benzoylheliotridine

Guidance literature:: With dmap; In acetonitrile; for 48h; Ambient temperature;
DOI:10.1021/jo00297a081

Reference yield:

: 126191-51-3
9-O-Benzoylheliotridine

: 126191-56-8
9-O-Benzoylsupinidine

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / 4-(dimethylamino)pyridine / acetonitrile / 48 h / Ambient temperature

2: 64 percent / 2,2'-azobis(2-methylpropionitrile), n-Bu₃SnH / toluene / 3 h / 75 °C

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; acetonitrile;
DOI:10.1021/jo00297a081