zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

Base Information

Chemical Name:zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine
CAS No.:97179-94-7
Molecular Formula:C₇₆H₄₄N₄Zn
Molecular Weight:1078.6
Hs Code.:

Synonyms:zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

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Technology Process of zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

There total 5 articles about zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 287410-99-5
[Zn(C₄NCH(CH₂)2CHC₆H₄C(C₆H₅))4]

: 97179-94-7
zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

Guidance literature:: In neat (no solvent); heated at 290°C in vac (10 mm Hg) for 10 min; elem. anal.;
DOI:10.1039/b002213f

Reference yield: 25.0%

: 103-82-2
phenylacetic acid

: 38119-07-2
3-acetyl-2-naphthoic acid

: 5970-45-6
zinc(II) acetate dihydrate

: 97179-94-7
zinc meso-tetraphenyltetra-2,3-naphthoporphine

Guidance literature:: In neat (no solvent); (He); kept (0.5 h, 360°C); cooled; ground; washed (hot water); dried; chromd. (Al2O3; CHCl3; chloroform-hexane-pyridine 30:10:1); elem.anal.;

Reference yield: 2.2%

: 103-82-2
phenylacetic acid

: 4379-54-8
2,3-Naphthalimide

: zinc(II) hydroxide

: 97179-94-7
zinc meso-tetraphenyltetra[2,3]naphthaloporphyrine

Guidance literature:: With H₂SO₄; In neat (no solvent); heating of a mixt. of reactants with a little conc. H2SO4 at 350-360°; resulting poduct was ground, washed with water, dried, dissolved in DMF,filtered through a bed of Al2O3, pptd. with aq.-alcoholic KOH; purified by chromy. on Al2O3, characterized by UV spectrum;