(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

Base Information

Chemical Name:(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine
CAS No.:1371586-79-6
Molecular Formula:C₄₃H₅₅NO₅
Molecular Weight:665.913
Hs Code.:

Synonyms:(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

Suppliers and Price of (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

There total 2 articles about (1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1371586-75-2
((1S,2R,3R,4S,5R,6R)-5-azido-6-(n-nonyloxy)cyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene

: 1371586-79-6
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

Guidance literature:: ((1S,2R,3R,4S,5R,6R)-5-azido-6-(n-nonyloxy)cyclohexane-1,2,3,4-tetrayl)tetrakis(oxy)tetrakis(methylene)tetrabenzene; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

With water; sodium sulfate; In tetrahydrofuran;
DOI:10.1021/jm300342q

Reference yield:

: 864948-63-0
(+)-(1R,2R,3S,4R,5R,6S)-2-azido-3,4,5,6-tetrakisbenzyloxycyclohexanol

: 1371586-79-6
(1R,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-(n-nonyloxy)cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm300342q