C₂₅H₃₂O₅Si

Base Information

Chemical Name:C₂₅H₃₂O₅Si
CAS No.:1447648-29-4
Molecular Formula:C₂₅H₃₂O₅Si
Molecular Weight:440.612
Hs Code.:

C<sub>25</sub>H<sub>32</sub>O<sub>5</sub>Si

Synonyms:C₂₅H₃₂O₅Si

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Chemical Property of C₂₅H₃₂O₅Si

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Technology Process of C₂₅H₃₂O₅Si

There total 1 articles about C₂₅H₃₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: C₂₅H₃₂O₆Si

: 1447648-29-4
C₂₅H₃₂O₅Si

: 1447648-30-7
C₂₅H₃₄O₆Si

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 2h; Molecular sieve; Inert atmosphere;
DOI:10.1002/asia.201300362

Reference yield:

: 1447648-29-4
C₂₅H₃₂O₅Si

: C₁₉H₁₈O₅

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/asia.201300362

Reference yield:

: 1447648-29-4
C₂₅H₃₂O₅Si

: polygalolide A

Guidance literature:: Multi-step reaction with 10 steps

1.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1.7 h / -10 - 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 1 h / 110 °C / Inert atmosphere

3.2: 16 h / 0 - 20 °C

4.1: iron(III) chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: manganese(IV) oxide / dichloromethane / 13 h / 20 °C / Inert atmosphere

6.1: caesium carbonate / methanol; tetrahydrofuran; water / 11 h / 0 °C / Inert atmosphere

7.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 0 °C

7.2: 6.6 h / 0 °C

8.1: ozone / dichloromethane / 0.25 h / -78 °C

8.2: 0.17 h / -78 °C / Inert atmosphere

9.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere

10.1: triethylamine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 7.5 h / 0 °C / Inert atmosphere

10.2: 0.67 h / -78 °C / Molecular sieve

With manganese(IV) oxide; iron(III) chloride; n-butyllithium; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; potassium carbonate; caesium carbonate; ozone; acetic acid; lithium tri-t-butoxyaluminum hydride; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 3.1: |Barton-McCombie Deoxygenation / 10.2: |Mukaiyama Aldol Addition;
DOI:10.1002/asia.201300362