C₃₄H₃₇NO

Base Information

Chemical Name:C₃₄H₃₇NO
CAS No.:1413301-84-4
Molecular Formula:C₃₄H₃₇NO
Molecular Weight:475.674
Hs Code.:

Synonyms:C₃₄H₃₇NO

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Chemical Property of C₃₄H₃₇NO

Chemical Property:

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Technology Process of C₃₄H₃₇NO

There total 5 articles about C₃₄H₃₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 872-85-5
pyridine-4-carbaldehyde

: 1413301-78-6
C₂₈H₃₃Br

: 1413301-84-4
C₃₄H₃₇NO

Guidance literature:: C₂₈H₃₃Br; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

pyridine-4-carbaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 4h; Inert atmosphere;

With manganese(IV) oxide; In chloroform; for 6h; Reflux; Inert atmosphere;
DOI:10.1039/c2dt31288c

Reference yield:

: 872-85-5
pyridine-4-carbaldehyde

: 1413301-78-6
C₂₈H₃₃Br

: 1413301-81-1
C₃₄H₃₉NO

: 1413301-84-4
C₃₄H₃₇NO

Guidance literature:: C₂₈H₃₃Br; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

pyridine-4-carbaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c2dt31288c

Reference yield:

: 939-97-9
4-tert-Butylbenzaldehyde

: 1413301-84-4
C₃₄H₃₇NO

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 4 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

1.3: 4 h / Reflux

2.1: sodium iodide; chloro-trimethyl-silane / hexane; acetonitrile / 6 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

3.2: 4 h / -78 °C / Inert atmosphere

With n-butyllithium; chloro-trimethyl-silane; sodium iodide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1039/c2dt31288c