C₂₄H₂₂ClN₅O₃S

Base Information

Chemical Name:C₂₄H₂₂ClN₅O₃S
CAS No.:1404117-37-8
Molecular Formula:C₂₄H₂₂ClN₅O₃S
Molecular Weight:495.989
Hs Code.:

C<sub>24</sub>H<sub>22</sub>ClN<sub>5</sub>O<sub>3</sub>S

Synonyms:C₂₄H₂₂ClN₅O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₂ClN₅O₃S

Chemical Property:

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Technology Process of C₂₄H₂₂ClN₅O₃S

There total 5 articles about C₂₄H₂₂ClN₅O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₂₉ClN₄O₆S

: 1404117-37-8
C₂₄H₂₂ClN₅O₃S

Guidance literature:: With ammonia; In tetrahydrofuran; dichloromethane; at -15 - 20 ℃;
DOI:10.1016/j.bmcl.2012.08.004

Reference yield:

: 59074-26-9
3-(4-chlorophenyl)-4-phenyl-4,5-dihydro-1H-pyrazole

: 1404117-37-8
C₂₄H₂₂ClN₅O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene / Reflux

2.1: phosphorus pentachloride / chlorobenzene / Reflux

3.1: triethylamine / dichloromethane / 20 °C / Cooling with ice

4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 20 °C

4.2: pH Ca_.2

5.1: 4-methyl-morpholine / dichloromethane / 0.42 h / -15 °C

6.1: ammonia / dichloromethane; tetrahydrofuran / -15 - 20 °C

With 4-methyl-morpholine; lithium hydroxide monohydrate; phosphorus pentachloride; ammonia; triethylamine; In tetrahydrofuran; dichloromethane; water; chlorobenzene; toluene;
DOI:10.1016/j.bmcl.2012.08.004

Reference yield:

: 1404117-68-5
C₂₅H₂₂ClN₃O₅S

: 1404117-37-8
C₂₄H₂₂ClN₅O₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: phosphorus pentachloride / chlorobenzene / Reflux

2.1: triethylamine / dichloromethane / 20 °C / Cooling with ice

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 20 °C

3.2: pH Ca_.2

4.1: 4-methyl-morpholine / dichloromethane / 0.42 h / -15 °C

5.1: ammonia / dichloromethane; tetrahydrofuran / -15 - 20 °C

With 4-methyl-morpholine; lithium hydroxide monohydrate; phosphorus pentachloride; ammonia; triethylamine; In tetrahydrofuran; dichloromethane; water; chlorobenzene;
DOI:10.1016/j.bmcl.2012.08.004