C₁₉H₂₅NO₃

Base Information

Chemical Name:C₁₉H₂₅NO₃
CAS No.:1309589-65-8
Molecular Formula:C₁₉H₂₅NO₃
Molecular Weight:315.412
Hs Code.:

C<sub>19</sub>H<sub>25</sub>NO<sub>3</sub>

Synonyms:C₁₉H₂₅NO₃

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Chemical Property of C₁₉H₂₅NO₃

Chemical Property:

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Technology Process of C₁₉H₂₅NO₃

There total 5 articles about C₁₉H₂₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1309589-64-7
C₁₉H₂₇NO₄

: 1309589-65-8
C₁₉H₂₅NO₃

Guidance literature:: With tetrachloromethane; 1-methylcyclohex-1-ene; TOP; In toluene; at 20 - 70 ℃; for 2h;
DOI:10.3987/COM-10-S(E)76

Reference yield:

: 1309589-62-5
C₂₂H₂₈O₄

: 1309589-65-8
C₁₉H₂₅NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 15 h / 0 - 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C / pH 8 / aq. buffer

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 0 °C

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate / dichloromethane / 3.5 h / 40 °C

4.2: 12 h / 20 °C

5.1: tetrachloromethane; 1-methylcyclohex-1-ene; TOP / toluene / 2 h / 20 - 70 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; tetrachloromethane; 1-methylcyclohex-1-ene; TOP; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Williamson etherification;
DOI:10.3987/COM-10-S(E)76

Reference yield:

: 1309589-63-6
C₂₆H₃₅NO₅

: 1309589-65-8
C₁₉H₂₅NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 °C / pH 8 / aq. buffer

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 0 °C

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate / dichloromethane / 3.5 h / 40 °C

3.2: 12 h / 20 °C

4.1: tetrachloromethane; 1-methylcyclohex-1-ene; TOP / toluene / 2 h / 20 - 70 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; tetrachloromethane; 1-methylcyclohex-1-ene; TOP; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.3987/COM-10-S(E)76