1,4-Dihexyloxy-2-methylbenzol

Base Information

• Chemical Name: 1,4-Dihexyloxy-2-methylbenzol
• CAS No.: 157202-49-8
• Molecular Formula: C₁₉H₃₂O₂
• Molecular Weight: 292.462
• Mol file: 157202-49-8.mol

Synonyms:1,4-Dihexyloxy-2-methylbenzol

Chemical Property of 1,4-Dihexyloxy-2-methylbenzol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-Dihexyloxy-2-methylbenzol

There total 1 articles about 1,4-Dihexyloxy-2-methylbenzol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-bromo-hexane (111-25-1) + 2-methylbenzene-1,4-diol (95-71-6,96937-50-7) → 1,4-Dihexyloxy-2-methylbenzol (157202-49-8)

Guidance literature:

With potassium hydroxide; Aliquat 336; In 1,2-dimethoxyethane; for 24h; Heating;

DOI:10.1002/prac.19943360311

Reference yield:

1,4-Dihexyloxy-2-methylbenzol (157202-49-8) → 2-bromomethyl-1,4-bis-hexyloxy-benzene

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane; Heating;

Reference yield:

1,4-Dihexyloxy-2-methylbenzol (157202-49-8) → E-2,6-Bis(α-cyano-2',5'-di-n-hexyloxystyryl)-1,5-di-n-hexyloxynaphthalene

Guidance literature:

Multi-step reaction with 3 steps

1: NBS / CCl₄ / Heating

2: CH₂Cl₂

3: 59 percent / Bu₄NOH; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.33 h / 40 °C

With N-Bromosuccinimide; potassium tert-butylate; tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane; tert-butyl alcohol; 1: Bromination / 2: Alkylation / 3: Knoevenagel condensation;

upstream raw materials:

1-bromo-hexane

2-methylbenzene-1,4-diol

Downstream raw materials:

2,5-Dihexyloxy-4-methylbenzaldehyd

2,5-dihexyloxybenzacetonitrile