[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester
CAS No.:160978-35-8
Molecular Formula:C₃₀H₄₂N₄O₆S₂
Molecular Weight:618.819
Hs Code.:

[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-<i>tert</i>-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid <i>tert</i>-butyl ester

Synonyms:[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

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Chemical Property of [1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

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Technology Process of [1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

There total 2 articles about [1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 160978-33-6
N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide

: 160978-35-8
[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: N^α-tert-butoxycarbonyl-S-allyloxycarbonylaminomethyl-L-cysteine benzylamide; With tri-n-butyl-tin hydride; acetic acid; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; at 20 ℃; for 0.5h;

With iodine; In tetrachloromethane;
DOI:10.1016/S0040-4020(99)00322-1

Reference yield:

: 10389-65-8
di-t-butoxycarbonyl-L-cystine

: 100-46-9
benzylamine

: 160978-35-8
[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide;
DOI:10.1002/chem.200304952

Reference yield:

: 814-68-6,25189-84-8
acryloyl chloride

: 160978-35-8
[1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester

: (N-Acr-L-Cys-NHBn)2

Guidance literature:: [1-benzylcarbamoyl-2-(2-benzylcarbamoyl-2-tert-butoxycarbonylamino-ethyldisulfanyl)-ethyl]-carbamic acid tert-butyl ester; With trifluoroacetic acid;

acryloyl chloride; pH=10.5; Further stages.;
DOI:10.1002/chem.200304952