phenyldimorpholinoiodophosphonium triiodide

Base Information

• Chemical Name: phenyldimorpholinoiodophosphonium triiodide
• CAS No.: 110523-92-7
• Molecular Formula: C₁₄H₂₁IN₂O₂P*I₃
• Molecular Weight: 787.925
• Mol file: 110523-92-7.mol

Synonyms:phenyldimorpholinoiodophosphonium triiodide

Chemical Property of phenyldimorpholinoiodophosphonium triiodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of phenyldimorpholinoiodophosphonium triiodide

There total 4 articles about phenyldimorpholinoiodophosphonium triiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

morpholinophenylphosphinous iodide (110523-88-1) → diphenyl phenylphosphonite (13410-61-2) + phenyldimorpholinoiodophosphonium triiodide (110523-92-7)

Guidance literature:

With iodine; In chlorobenzene; benzene; for 0.166667h; Yields of byproduct given; Heating;

Reference yield: 95.0%

4-(trimethylsilyl)morpholine (13368-42-8) + phenyltetraiodophosphorane (26852-27-7) → phenyldimorpholinoiodophosphonium triiodide (110523-92-7) + diiodo-phenylphosphine (20472-19-9)

Guidance literature:

In chlorobenzene; benzene; at 80 ℃; for 0.166667h; other substrates, other Si-compounds;

Reference yield:

diiodo-phenylphosphine (20472-19-9) → phenyldimorpholinoiodophosphonium triiodide (110523-92-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / benzene / 1 h / 20 °C

2: 1.) I₂ / 1.) benzene, chlorobenzene, 10 min, reflux; 2.) benzene, chlorobenzene, 30 min, reflux

With iodine; In benzene;

upstream raw materials:

4-(trimethylsilyl)morpholine

phenyltetraiodophosphorane

sodium phenoxide

morpholinophenylphosphinous iodide