(S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

Base Information

Chemical Name:(S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide
CAS No.:117653-13-1
Molecular Formula:2BrH*C₂₂H₂₀I₂N₂O₄
Molecular Weight:792.045
Hs Code.:

Synonyms:(S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

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Chemical Property of (S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

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Technology Process of (S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

There total 8 articles about (S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92199-93-4
1-methoxy-2-(4-nitrobenzyl)benzene

: 117653-13-1
(S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

2: 1) MX, 2) Cu bronze, Et₃N

3: H₂ / sulfided Pt/C

4: HBr, AcOH / H₂O

With copper bronze; hydrogen bromide; hydrogen; acetic acid; triethylamine; sulfided Pt/C; In water;
DOI:10.1021/jm00122a009

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 117653-13-1
(S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

Guidance literature:: Multi-step reaction with 6 steps

2: Et₃SiH, CF₃CO₂H

4: 1) MX, 2) Cu bronze, Et₃N

5: H₂ / sulfided Pt/C

6: HBr, AcOH / H₂O

With triethylsilane; copper bronze; hydrogen bromide; hydrogen; acetic acid; triethylamine; trifluoroacetic acid; sulfided Pt/C; In water;
DOI:10.1021/jm00122a009

Reference yield:

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 117653-13-1
(S)-2-Amino-3-{4-[3-(4-amino-benzyl)-4-hydroxy-phenoxy]-3,5-diiodo-phenyl}-propionic acid; hydrobromide

Guidance literature:: Multi-step reaction with 6 steps

2: Et₃SiH, CF₃CO₂H

4: 1) MX, 2) Cu bronze, Et₃N

5: H₂ / sulfided Pt/C

6: HBr, AcOH / H₂O

With triethylsilane; copper bronze; hydrogen bromide; hydrogen; acetic acid; triethylamine; trifluoroacetic acid; sulfided Pt/C; In water;
DOI:10.1021/jm00122a009