6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol

Base Information

• Chemical Name: 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol
• CAS No.: 140391-29-3
• Molecular Formula: C₄₅H₅₅N₃O₁₀
• Molecular Weight: 797.946

Synonyms:6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol

Chemical Property of 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol

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Technology Process of 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol

There total 4 articles about 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-2,3:4,5-di-O-cyclohexylidene-1-O-(1R)-menthyloxycarbonyl-D-myo-inositol → 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol (140391-29-3)

Guidance literature:

With potassium carbonate; In methanol; dichloromethane; at 40 ℃; for 48h;

DOI:10.1002/(SICI)1099-0690(199802)1998:2<291::AID-EJOC291>3.0.CO;2-6

Reference yield: 95.0%

C56H73N3O12 (202812-15-5) → 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol (140391-29-3)

Guidance literature:

With potassium carbonate; In methanol; at 40 ℃;

Reference yield: 75.0%

6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-1-O-camphanyl-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol → 6-O-(2-Azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3:4,5-di-O-cyclohexylidene-D-myo-inositol (140391-29-3)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; for 0.5h;

DOI:10.1021/jo00035a015

upstream raw materials:

C₅₆H₇₃N₃O₁₂

C₅₂H₅₉N₃O₁₁

Downstream raw materials:

O-2-amino-2-deoxy-α-D-glucopyranosyl (1-6)-D-myo-inositol

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