2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide

Base Information

Chemical Name:2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide
CAS No.:605681-59-2
Molecular Formula:C₁₇H₁₇ClN₄O₂
Molecular Weight:344.801
Hs Code.:

Synonyms:2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide

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Chemical Property of 2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide

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Technology Process of 2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide

There total 2 articles about 2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4144-64-3
2-(1H-1,2,3-benzotriazol-1-yl)acetic acid

: 605681-59-2
2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.42 h / -78 °C

2.2: 6 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;

Reference yield:

: 605681-58-1
2-(1H-1,2,3-benzotriazol-1-yl)-N-methoxy-N-methylacetamide

: 622-95-7
4-chlorobenzyl bromide

: 605681-59-2
2-(1H-1,2,3-benzotriazol-1-yl)-3-(4-chlorophenyl)-N-methoxy-N-methyl-propanamide

Guidance literature:: 2-(1H-1,2,3-benzotriazol-1-yl)-N-methoxy-N-methylacetamide; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.416667h;

4-chlorobenzyl bromide; In tetrahydrofuran; at -78 - 20 ℃; for 6h;