[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

Base Information

Chemical Name:[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate
CAS No.:1238892-35-7
Molecular Formula:C₃₁H₃₆BrNO₉
Molecular Weight:646.532
Hs Code.:

Synonyms:[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

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Technology Process of [8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

There total 1 articles about [8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 103-82-2
phenylacetic acid

: 1221557-62-5
8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-4-(chloromethyl)-7-hydroxycoumarin

: 1238892-35-7
[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 2h; Inert atmosphere; Darkness; Reflux;
DOI:10.1021/jo100368w

Reference yield: 95.0%

: 1238892-35-7
[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

: 1221557-58-9
[8-[bis(carboxymethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl phenylacetate

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 - 40 ℃; for 1.5h; Inert atmosphere; Darkness;
DOI:10.1021/jo100368w