trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate

Base Information

• Chemical Name: trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate
• CAS No.: 82938-79-2
• Molecular Formula: C₃₃H₄₄N₂O₄S*ClH
• Molecular Weight: 601.25

Synonyms:trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate

Chemical Property of trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate

Chemical Property:

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Technology Process of trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate

There total 46 articles about trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-[(4aR,8S,8aS)-4a-Benzyl-8-{[(S)-2-tert-butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionylamino]-methyl}-octahydro-naphthalen-(2E)-ylidene]-4-methylsulfanyl-butyric acid methyl ester (82938-75-8) → trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate (82938-79-2)

Guidance literature:

With hydrogenchloride; In chloroform; for 1h; Ambient temperature;

DOI:10.1139/v82-151

Reference yield: 80.0%

2-[(4aS,8R,8aR)-4a-Benzyl-8-{[(R)-2-tert-butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionylamino]-methyl}-octahydro-naphthalen-(2E)-ylidene]-4-methylsulfanyl-butyric acid methyl ester (82938-75-8,82938-76-9,82938-77-0,82938-78-1) → trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)-2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate (82938-79-2,82938-80-5,82938-81-6,82938-82-7)

Guidance literature:

With hydrogenchloride; In chloroform; for 1h; Ambient temperature;

DOI:10.1139/v82-151

Reference yield: 54.0%

2-[(4aS,8R,8aR)-4a-Benzyl-8-{[(R)-2-tert-butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionylamino]-methyl}-octahydro-naphthalen-(2Z)-ylidene]-4-methylsulfanyl-butyric acid methyl ester (82938-75-8,82938-76-9,82938-77-0,82938-78-1) → trans-methyl-2-(decahydro-4β-(phenylmethyl)-8β-(L-tyrosylaminomethyl)-2-naphthalenylidene)-4-(methylthio)butanoate HCl monohydrate (82938-79-2,82938-80-5,82938-81-6,82938-82-7)

Guidance literature:

With hydrogenchloride; In chloroform; for 1h; Ambient temperature;

DOI:10.1139/v82-151

upstream raw materials:

2-[(4aR,8S,8aS)-4a-Benzyl-8-{[(S)-2-tert-butoxycarbonylamino-3-(4-hydroxy-phenyl)-propionylamino]-methyl}-octahydro-naphthalen-(2E)-ylidene]-4-methylsulfanyl-butyric acid methyl ester

4-Methylsulfanyl-2-trimethylsilanyl-butyric acid

methyl 2-trimethylsilyl-4-methylthiobutyrate

1,2,3,5,6,7,8,8a-octahydro-3-oxo-8a-phenylmethylnaphthalene

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