(S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

Base Information

Chemical Name:(S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate
CAS No.:1423218-81-8
Molecular Formula:C₂₅H₂₈N₂O₄S
Molecular Weight:452.574
Hs Code.:

Synonyms:(S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

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Chemical Property of (S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

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Technology Process of (S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

There total 6 articles about (S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 624-31-7
4-tolyl iodide

: 1384331-68-3
(S)-mehyl 3-mehyl-2-(pyridine-2-sulfonamido)butanoate

: 1423218-81-8
(S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

Guidance literature:: With silver(I) acetate; palladium diacetate; at 150 ℃; for 4h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.9b01523

Reference yield: 70.0%

: 624-31-7
4-tolyl iodide

: 1384331-68-3
(S)-mehyl 3-mehyl-2-(pyridine-2-sulfonamido)butanoate

: 1423218-79-4
(2S,3S)-mehyl 3-mehyl-2-(pyridine-2-sulfonamido)-4-(p-tolyl)butanoate

: 1423218-81-8
(S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

Guidance literature:: With 1,1,1,3',3',3'-hexafluoro-propanol; silver(I) acetate; palladium diacetate; at 150 ℃; for 4h; stereoselective reaction;
DOI:10.1039/c2sc21162a

Reference yield:

: 6306-52-1
L-valine methylester hydrochloride

: 1423218-81-8
(S)-mehyl 3-(4-mehylbenzyl)-2-(pyridine-2-sulfonamido)-4-(p-tolyl)-butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N,N,N,-tetramethylethylenediamine / acetonitrile / 16 h / 20 °C

2: 1,1,1,3',3',3'-hexafluoro-propanol; palladium diacetate; silver(I) acetate / 4 h / 150 °C

With N,N,N,N,-tetramethylethylenediamine; 1,1,1,3',3',3'-hexafluoro-propanol; silver(I) acetate; palladium diacetate; In acetonitrile;
DOI:10.1039/c2sc21162a