(2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

Base Information

Chemical Name:(2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate
CAS No.:1255910-65-6
Molecular Formula:C₃₂H₄₂O₄Si
Molecular Weight:518.769
Hs Code.:

Synonyms:(2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

Suppliers and Price of (2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

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Technology Process of (2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

There total 1 articles about (2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1255910-64-5
(2S,6R,E)-7-(tert-butyldimethylsilyloxy)-2-hydroxy-2,6-dimethylhept-3-enyl benzoate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1255910-65-6
(2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

Guidance literature:: (2S,6R,E)-7-(tert-butyldimethylsilyloxy)-2-hydroxy-2,6-dimethylhept-3-enyl benzoate; With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 16h;

In methanol; at 20 ℃; for 2h; Inert atmosphere;

tert-butylchlorodiphenylsilane; With 1H-imidazole; dmap; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol102177j

Reference yield: 85.0%

: 1255910-65-6
(2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate

: 1255910-66-7
C₂₅H₃₈O₃Si

Guidance literature:: (2S,6R)-7-(tert-butyldiphenylsilyloxy)-2-hydroxy-2,6-dimethylheptyl benzoate; With methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 2h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ol102177j