1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene

Base Information

• Chemical Name: 1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene
• CAS No.: 1422444-58-3
• Molecular Formula: C₁₂H₁₁F₇O₃
• Molecular Weight: 336.206
• Mol file: 1422444-58-3.mol

Synonyms:1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene

Chemical Property of 1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene

There total 2 articles about 1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,2,3-trimethoxybenzene (621-23-8) + 1,1,1,2,2,3,3-heptafluoro-3-iodo-propane (754-34-7) → 1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene (1422444-58-3)

Guidance literature:

1,2,3-trimethoxybenzene; With C₅₂H₇₃CoN₄O₁₄⁽¹⁺⁾*ClO₄^(1-); tetrabutylammonium perchlorate; In methanol; Irradiation; Inert atmosphere; Electrolysis;

1,1,1,2,2,3,3-heptafluoro-3-iodo-propane; In methanol; for 9h; Solvent; Catalytic behavior; Electrolysis; Inert atmosphere;

DOI:10.1039/c7cc06221d

Reference yield: 83.0%

1,2,3-trimethoxybenzene (621-23-8) + sodium perfluoropropylsulfinate (152893-99-7) → 1,3,5-trimethoxy-2-(1,1,2,2,3,3,3-heptafluoropropyl)benzene (1422444-58-3)

Guidance literature:

With anthraquinone-2-carboxylic acid; trifluoroacetic acid; In acetonitrile; at 20 ℃; for 60h; Inert atmosphere; Irradiation;

DOI:10.1002/adsc.201300199

upstream raw materials:

1,2,3-trimethoxybenzene

sodium perfluoropropylsulfinate

1,1,1,2,2,3,3-heptafluoro-3-iodo-propane