N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide

Base Information

• Chemical Name: N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide
• CAS No.: 906560-94-9
• Molecular Formula: C₃₄H₃₆Br₂N₄O₄
• Molecular Weight: 724.492

Synonyms:N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide

Chemical Property of N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide

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Technology Process of N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide

There total 2 articles about N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(2-{{3-[allyl-(4-bromo-phenyl)-carbamoyl]-propionyl}-[2-(4-bromo-phenyl)-ethyl]-amino}-2-phenyl-acetylamino)-acetic acid ethyl ester (906560-78-9) + 1-amino-2-propene (107-11-9,30551-89-4) → N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide (906560-94-9)

Guidance literature:

In ethanol; at 40 ℃; for 36h;

DOI:10.1016/j.tetlet.2006.04.098

Reference yield:

(2-{[3-(4-bromo-phenylcarbamoyl)-propionyl]-[2-(4-bromo-phenyl)-ethyl]-amino}-2-phenyl-acetylamino)-acetic acid ethyl ester → N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide (906560-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 39 percent / Cs₂CO₃ / dimethylformamide / 24 h / 20 °C

2: 91 percent / ethanol / 36 h / 40 °C

With caesium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2006.04.098

Reference yield: 62.0%

N-allyl-N'-[(allylcarbamoylmethyl-carbamoyl)-phenyl-methyl]-N-(4-bromo-phenyl)-N'-[2-(4-bromo-phenyl)-ethyl]-succinamide (906560-94-9) → (E)-12-(4-Bromo-phenyl)-7-[2-(4-bromo-phenyl)-ethyl]-6-phenyl-1,4,7,12-tetraaza-cyclohexadec-14-ene-2,5,8,11-tetraone

Guidance literature:

[1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; In 1,2-dichloro-ethane; at 60 ℃; for 8h;

DOI:10.1016/j.tetlet.2006.04.098

upstream raw materials:

(2-{{3-[allyl-(4-bromo-phenyl)-carbamoyl]-propionyl}-[2-(4-bromo-phenyl)-ethyl]-amino}-2-phenyl-acetylamino)-acetic acid ethyl ester

1-amino-2-propene

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