N₁-phenyl-1,2-butanediamine

Base Information

• Chemical Name: N₁-phenyl-1,2-butanediamine
• CAS No.: 854459-39-5
• Molecular Formula: C₁₀H₁₆N₂
• Molecular Weight: 164.25
• Mol file: 854459-39-5.mol

Synonyms:N₁-phenyl-1,2-butanediamine

Chemical Property of N₁-phenyl-1,2-butanediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₁-phenyl-1,2-butanediamine

There total 2 articles about N₁-phenyl-1,2-butanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-aminobutanol (96-20-8,13054-87-0) + aniline (62-53-3) → N1-phenyl-1,2-butanediamine (854459-39-5)

Guidance literature:

With [RuCl(N,N-dimethyl-1-[6-(4'-methylphenyl)pyridin-2-yl]methaneamine(-H))(dppb)]; potassium tert-butylate; In tetrahydrofuran; toluene; at 110 ℃; for 24h; Inert atmosphere; Molecular sieve;

DOI:10.1021/ol3001969

Reference yield:

2-ethylaziridine (2549-67-9) + aniline (62-53-3) → N1-phenyl-1,2-butanediamine (854459-39-5) + 1-ethyl-N1-phenyl-ethanediyldiamine

Guidance literature:

With ammonium chloride;

DOI:10.1021/ja01181a053

Reference yield:

N1-phenyl-1,2-butanediamine (854459-39-5) → 2-benzoylamino-1-(N-benzoyl-anilino)-butane

Guidance literature:

DOI:10.1021/ja01181a053

upstream raw materials:

2-ethylaziridine

aniline

2-aminobutanol