1,5-di-o-tolyl-thio carbonohydrazide

Base Information

Chemical Name:1,5-di-o-tolyl-thio carbonohydrazide
CAS No.:92871-89-1
Molecular Formula:C₁₅H₁₈N₄S
Molecular Weight:286.401
Hs Code.:

1,5-di-<i>o</i>-tolyl-thio carbonohydrazide

Synonyms:1,5-di-o-tolyl-thio carbonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,5-di-o-tolyl-thio carbonohydrazide

Chemical Property:

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Technology Process of 1,5-di-o-tolyl-thio carbonohydrazide

There total 4 articles about 1,5-di-o-tolyl-thio carbonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28101-05-5
3-nitro-1,5-di-o-tolyl-3-nitroformazan

: 92871-89-1
1,5-di-o-tolyl-thio carbonohydrazide

Guidance literature:: With diammonium sulfide; In ethanol; water; at 35 ℃; for 0.333333h;
DOI:10.1016/j.jphotochem.2012.11.009

Reference yield:

: 28101-05-5,80991-21-5
3-Nitro-1,5-di-o-tolyl-formazan

: 92871-89-1
1,5-di-o-tolyl-thio carbonohydrazide

Guidance literature:: With ethanol; hydrogen sulfide; ammonia;
DOI:10.1021/ja01252a042

Reference yield:

: 95-53-4
o-toluidine

: 92871-89-1
1,5-di-o-tolyl-thio carbonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0.5 h / 0 °C

1.2: 2 h / 20 °C

2.1: diammonium sulfide / ethanol; water / 0.33 h / 35 °C

With hydrogenchloride; diammonium sulfide; sodium nitrite; In ethanol; water;
DOI:10.1016/j.jphotochem.2012.11.009