4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine

Base Information

• Chemical Name: 4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine
• CAS No.: 1142360-65-3
• Molecular Formula: C₂₆H₁₈F₂N₆O₄S₂
• Molecular Weight: 580.596

Synonyms:4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine

Chemical Property of 4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine

Chemical Property:

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Technology Process of 4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine

There total 1 articles about 4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4,6-Dichloro-2-(methylthio)pyrimidine (6299-25-8) + 4,6-bis(3-hydroxyphenoxy)pyrimidine (1142360-46-0) → 4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine (1142360-65-3)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol900116h

Reference yield: 77.0%

4,6-bis(3-hydroxy-5-methylphenoxy)-2-phenylpyrimidine (1142360-50-6) + 4,6-bis[3-(6-fluoro-2-methylsulfanylpyrimidin-4-yloxy)phenoxy]pyrimidine (1142360-65-3) → 4,6,16,18,28,30,40,42-octaaza-5,29-bis(methylsulfanyl)-11,23-dimethyl-17-phenyl-2,8,14,20,26,32,38,44-octaoxacalix[8]arene (1142360-68-6)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In 1,4-dioxane; for 6h; Reflux;

DOI:10.1021/ol900116h

upstream raw materials:

4,6-Dichloro-2-(methylthio)pyrimidine

4,6-bis(3-hydroxyphenoxy)pyrimidine

Downstream raw materials:

4,6,16,18,28,30,40,42-octaaza-5,29-bis(methylsulfanyl)-11,23-dimethyl-17-phenyl-2,8,14,20,26,32,38,44-octaoxacalix[8]arene

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