2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

Base Information

Chemical Name:2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone
CAS No.:111075-26-4
Molecular Formula:C₂₇H₃₂O₃
Molecular Weight:404.549
Hs Code.:

Synonyms:2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

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Chemical Property of 2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

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Technology Process of 2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

There total 5 articles about 2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 111075-25-3
2-<7-(3-methoxyphenyl)-6-(phenylmethoxymethyl)-4-(E)-heptenyl>-5-methyl-furan

: 111075-26-4
2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

Guidance literature:: With sulfuric acid; In water; acetic acid; for 3h; Heating;
DOI:10.1002/recl.19861051206

Reference yield:

: 61227-48-3
[(3-methoxyphenyl)methyl]propanedioic acid diethyl ester

: 111075-26-4
2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

Guidance literature:: Multi-step reaction with 5 steps

1: 71.5 percent / lithium aluminum hydride / diethyl ether / 2 h / 20 °C

2: 82 percent / THF, HMPA, sodium hydride / paraffin / 7 h / Ambient temperature

3: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

4: 1.) phenyllithium / 1.) THF, ether, 10 min, -60 deg C, 2.) THF, ether, 15 min, -30 deg C

5: 89 percent / 4 N sulphuric acid / H₂O; acetic acid / 3 h / Heating

With tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sulfuric acid; sodium hydride; phenyllithium; pyridinium chlorochromate; In diethyl ether; dichloromethane; water; acetic acid; paraffin;
DOI:10.1002/recl.19861051206

Reference yield:

: 77756-13-9
2-<(3-methoxyphenyl)methyl>-1,3-propanediol

: 111075-26-4
2-<6-(3-methoxyphenyl)-5-(phenylmethoxymethyl)-3-(E)-hexenyl>-3-methyl-2-methyl-2-cyclopentenone

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / THF, HMPA, sodium hydride / paraffin / 7 h / Ambient temperature

2: 82 percent / pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

3: 1.) phenyllithium / 1.) THF, ether, 10 min, -60 deg C, 2.) THF, ether, 15 min, -30 deg C

4: 89 percent / 4 N sulphuric acid / H₂O; acetic acid / 3 h / Heating

With tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; sulfuric acid; sodium hydride; phenyllithium; pyridinium chlorochromate; In dichloromethane; water; acetic acid; paraffin;
DOI:10.1002/recl.19861051206