1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene

Base Information

Chemical Name:1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene
CAS No.:1049822-86-7
Molecular Formula:C₄₀H₃₄O₄S₄
Molecular Weight:706.972
Hs Code.:

Synonyms:1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene

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Chemical Property of 1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene

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Technology Process of 1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene

There total 1 articles about 1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1049822-46-9
1,4-bis(5-bromo-2-thienyl)-2,5-bis(3-methyl-2-thienyl)benzene

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 1049822-86-7
1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; for 3h; Reflux; Inert atmosphere;
DOI:10.1021/ol801828n

Reference yield:

: 1049822-86-7
1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene

: C₄₀H₃₃IO₄S₄

: 1049822-91-4
1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(5-iodo-3-methyl-2-thienyl)benzene

Guidance literature:: 1,4-bis[5-(1,2-dimethoxy-4-phenyl)-2-thienyl]-2,5-bis(3-methyl-2-thienyl)benzene; With mercury(II) diacetate; acetic acid; In dichloromethane; at 20 ℃; for 1h; Darkness;

With iodine; In dichloromethane; acetic acid; at 20 ℃; for 24h;
DOI:10.1021/ol801828n