3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea

Base Information

• Chemical Name: 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea
• CAS No.: 935439-72-8
• Molecular Formula: C₁₈H₁₃F₃N₂O₂S
• Molecular Weight: 378.375

Synonyms:3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea

Chemical Property of 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea

Chemical Property:

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Technology Process of 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea

There total 1 articles about 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoro-N-methyl-4-(2-propynylthio)-aniline (935440-49-6) + 2,6-difluorobenzoyl isocyanate (60731-73-9) → 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea (935439-72-8)

Guidance literature:

In diethyl ether; at 20 ℃; for 17h;

Reference yield:

3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea (935439-72-8) → 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylsulfinyl)-phenyl]-1-methyl-urea

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; water; at 0 ℃; for 0.5h;

Reference yield:

3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylthio)-phenyl]-1-methyl-urea (935439-72-8) → 3-(2,6-difluorobenzoyl)-1-[2-fluoro-4-(2-propynylsulfonyl)-phenyl]-1-methyl-urea

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; water; at 20 ℃; for 2h;

upstream raw materials:

2-fluoro-N-methyl-4-(2-propynylthio)-aniline

2,6-difluorobenzoyl isocyanate

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