4-methylresorcinol diacetate

Base Information

• Chemical Name: 4-methylresorcinol diacetate
• CAS No.: 71119-00-1
• Molecular Formula: C₁₁H₁₂O₄
• Molecular Weight: 208.214
• Mol file: 71119-00-1.mol

Synonyms:4-methylresorcinol diacetate

Chemical Property of 4-methylresorcinol diacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-methylresorcinol diacetate

There total 5 articles about 4-methylresorcinol diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.2%

2,4-Dihydroxybenzaldehyde (95-01-2) → Resorcinol diacetate (108-58-7) + 4,6-dimethylresorcinol diacetate (15536-79-5) + 4-methylresorcinol diacetate (71119-00-1)

Guidance literature:

With sodium hydroxide; sodium tetrahydroborate; In water; at 100 ℃; Product distribution; after acetylation;

Reference yield:

4-hydroxy-4-methyl-cyclohexa-2,5-dienone (23438-23-5) + acetic anhydride (108-24-7) → 4-methylresorcinol diacetate (71119-00-1)

Guidance literature:

With sulfuric acid;

DOI:10.1021/ja01558a049

Reference yield:

6,6'-dimethyl-4,4'-methanediyl-di-resorcinol → 4-methylresorcinol diacetate (71119-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH-solution; zinc dust

With sodium hydroxide; zinc;

upstream raw materials:

4-methyl resorcinol

acetic anhydride

4-acetoxy-4-methyl-2,5-cyclohexanedienone

4-hydroxy-4-methyl-cyclohexa-2,5-dienone

Downstream raw materials:

4-methyl resorcinol