5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Base Information

Chemical Name:5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione
CAS No.:82891-27-8
Molecular Formula:C₁₉H₁₈O₃S
Molecular Weight:326.416
Hs Code.:

Synonyms:5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Suppliers and Price of 5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

There total 5 articles about 5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 82891-21-2
(5aS,9aR,9bS)-9a-Hydroxy-5a-methyl-3-phenylsulfanyl-5,5a,8,9,9a,9b-hexahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

: 82891-27-8
5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Guidance literature:: With thionyl chloride; In pyridine; at 0 ℃; for 0.5h;
DOI:10.1021/ja00384a053

Reference yield:

: 1193-55-1
2-methylcyclohexane-1,3-dione

: 82891-27-8
5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / KF / dimethylsulfoxide; 1,2-dimethoxy-ethane / 1 h / 0 °C

2: 90 percent / thionyl chloride / pyridine / 0.5 h / 0 °C

With potassium fluoride; thionyl chloride; In pyridine; 1,2-dimethoxyethane; dimethyl sulfoxide;
DOI:10.1021/ja00384a053

Reference yield:

: 81470-07-7
α-(phenylthio)-β-vinylbutenolide

: 82891-27-8
5a-Methyl-3-phenylsulfanyl-5,5a,8,9-tetrahydro-4H,7H-naphtho[1,2-b]furan-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / KF / dimethylsulfoxide; 1,2-dimethoxy-ethane / 1 h / 0 °C

2: 90 percent / thionyl chloride / pyridine / 0.5 h / 0 °C

With potassium fluoride; thionyl chloride; In pyridine; 1,2-dimethoxyethane; dimethyl sulfoxide;
DOI:10.1021/ja00384a053