1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane

Base Information

• Chemical Name: 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane
• CAS No.: 85175-79-7
• Molecular Formula: C₂₄H₃₁Cl₂N₃O₃
• Molecular Weight: 480.434

Synonyms:1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane

Chemical Property of 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane

Chemical Property:

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Technology Process of 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane

There total 3 articles about 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4-amino-3,5-dichloro-phenyl}-ethyl)-amino]-propane (85175-98-0) → 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane (85175-79-7)

Guidance literature:

With hydrogen; palladium; In acetic acid;

Reference yield:

N-methyl-N-[2-(4-amino-3,5-dichloro-phenyl)-ethyl]-amine (85175-99-1) + 7,8-dimethoxy-3-(3-chloropropyl)-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one (85175-65-1) → 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane (85175-79-7)

Guidance literature:

Reference yield:

2-(4-amino-3,5-dichlorophenyl)-ethyl chloride (85175-91-3) + 7,8-dimethoxy-3-<3-(methylamino)propyl>-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one (85175-77-5) → 1-[7,8-dimethoxy-1,3,4,5,-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4amino-3,5-dichloro-phenyl}ethyl)-amino]-propane (85175-79-7)

Guidance literature:

upstream raw materials:

N-methyl-N-[2-(4-amino-3,5-dichloro-phenyl)-ethyl]-amine

7,8-dimethoxy-3-(3-chloropropyl)-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

2-(4-amino-3,5-dichlorophenyl)-ethyl chloride

7,8-dimethoxy-3-<3-(methylamino)propyl>-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

Downstream raw materials:

1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4-ethoxycarbonylamino-3,5-dichloro-phenyl}-ethyl)-amino]-propane

1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4-bis-(ethoxycarbonyl)-amino-3,5-dichlorophenyl}-ethyl)-amino]-propane

1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4-acetylamino-3,5-dichloro-phenyl}-ethyl)-amino]-propane

1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{4-dimethylamino-3,5-dichloro-phenyl}-ethyl)-amino]-propane

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