2-iodophenyl 6-bromohexanoate

Base Information

• Chemical Name: 2-iodophenyl 6-bromohexanoate
• CAS No.: 1259387-83-1
• Molecular Formula: C₁₂H₁₄BrIO₂
• Molecular Weight: 397.05
• Mol file: 1259387-83-1.mol

Synonyms:2-iodophenyl 6-bromohexanoate

Chemical Property of 2-iodophenyl 6-bromohexanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-iodophenyl 6-bromohexanoate

There total 1 articles about 2-iodophenyl 6-bromohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

6-bromohexanoyl chloride (22809-37-6) + 2-Iodophenol (533-58-4) → 2-iodophenyl 6-bromohexanoate (1259387-83-1)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1515/znb-2010-0912

Reference yield: 74.0%

2-iodophenyl 6-bromohexanoate (1259387-83-1) → 2-iodophenyl 6-iodohexanoate (1259387-86-4)

Guidance literature:

With sodium iodide; In acetone; at 50 ℃; for 16h;

DOI:10.1515/znb-2010-0912

Reference yield:

2-iodophenyl 6-bromohexanoate (1259387-83-1) → 2-iodophenyl 6-fluorohexanoate (1259387-90-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium iodide / acetone / 16 h / 50 °C

2: silver fluoride / acetonitrile / 16 h / 20 °C / Inert atmosphere; Darkness

With silver fluoride; sodium iodide; In acetone; acetonitrile;

DOI:10.1515/znb-2010-0912

upstream raw materials:

6-bromohexanoyl chloride

2-Iodophenol

Downstream raw materials:

2-iodophenyl 6-iodohexanoate

2-iodophenyl 6-fluorohexanoate