ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

Base Information

Chemical Name:ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate
CAS No.:440339-10-6
Molecular Formula:C₁₈H₁₉N₅O₂
Molecular Weight:337.381
Hs Code.:

Synonyms:ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

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Chemical Property of ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

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Technology Process of ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

There total 3 articles about ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 94-05-3,42466-69-3
ethyl (ethoxymethylene)cyanoacetate

: 440339-04-8
2-amino-1-isopropylideneamino-4-phenyl-1H-imidazole

: 440339-10-6
ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

Guidance literature:: In acetone; at 20 ℃; for 24h;
DOI:10.1002/jhet.5570390123

Reference yield: 20.0%

: 94-05-3,42466-69-3
ethyl (ethoxymethylene)cyanoacetate

: 440339-04-8
2-amino-1-isopropylideneamino-4-phenyl-1H-imidazole

: ethyl (1-amino-4-phenylimidazol-2-yl)aminomethylenecyanoacetate

: 440339-10-6
ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

Guidance literature:: In acetone; for 0.5h; Heating;
DOI:10.1002/jhet.5570390123

Reference yield:

: 15970-40-8
1,2-diamino-4-phenyl[1H]imidazole

: 440339-10-6
ethyl (4-phenyl-1-isopropylideneaminoimidazol-2-yl)aminomethylenecyanoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / acetic acid / ethanol / 2 h / Heating

2: 37 percent / acetone / 0.5 h / Heating

With acetic acid; In ethanol; acetone;
DOI:10.1002/jhet.5570390123