5-phenylhexanonitrile

Base Information

• Chemical Name: 5-phenylhexanonitrile
• CAS No.: 36603-29-9
• Molecular Formula: C₁₂H₁₅N
• Molecular Weight: 173.258

Synonyms:5-phenylhexanonitrile

Chemical Property of 5-phenylhexanonitrile

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of 5-phenylhexanonitrile

There total 3 articles about 5-phenylhexanonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

(E)-(pent-3-en-2-yl)benzene (42461-65-4) + 1-methylcyclohexa-2,5-diene-1-carbonitrile → 5-phenylhexanonitrile (36603-29-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tris(pentafluorophenyl)borate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; at 110 ℃; for 40h; regioselective reaction; Glovebox; Inert atmosphere;

DOI:10.1021/jacs.8b10651

Reference yield: 30.0%

3-phenyl-1-butanol (2722-36-3) + acetonitrile (75-05-8,26809-02-9) → 5-phenylhexanonitrile (36603-29-9)

Guidance literature:

3-phenyl-1-butanol; acetonitrile; With caesium carbonate; at 180 ℃; for 0.333333h; Microwave irradiation; Inert atmosphere;

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; at 180 ℃; for 12h; Microwave irradiation; Inert atmosphere;

DOI:10.1021/ol2015972

Reference yield:

6-chlorohexanenitrile (6628-78-0) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 6-phenylhexanenitrile (17777-31-0) + 5-phenylhexanonitrile (36603-29-9)

Guidance literature:

With aluminium trichloride; Product distribution; degree of isomerization of the alkyl chain;

DOI:10.1007/BF00959375

upstream raw materials:

6-chlorohexanenitrile

benzene

3-phenyl-1-butanol

acetonitrile

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