Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Base Information

• Chemical Name: Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine
• CAS No.: 1026516-87-9
• Molecular Formula: C₂₇H₃₈N₂O₂
• Molecular Weight: 422.611

Synonyms:Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Chemical Property of Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

Chemical Property:

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Technology Process of Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine

There total 3 articles about Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromobenzene (108-86-1,52753-63-6) → Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine (1026516-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate, copper iodide / xylene / 19 h / 150 °C

2: 1.) NaH / 1.) DMF, 1 h, 2.) DMF, 1 h

With copper(l) iodide; sodium hydride; potassium carbonate; In xylene;

DOI:10.1021/jm9704309

Reference yield:

5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-3-nitro-2-naphthylamine (155877-70-6) → Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine (1026516-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate, copper iodide / xylene / 19 h / 150 °C

2: 1.) NaH / 1.) DMF, 1 h, 2.) DMF, 1 h

With copper(l) iodide; sodium hydride; potassium carbonate; In xylene;

DOI:10.1021/jm9704309

Reference yield:

1-Iodoheptane (4282-40-0) + (5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-3-nitro-2-naphthyl)phenylamine (155877-75-1) → Heptyl-phenyl-(5,5,8,8-tetramethyl-3-nitro-5,6,7,8-tetrahydro-naphthalen-2-yl)-amine (1026516-87-9)

Guidance literature:

With sodium hydride; Multistep reaction; 1.) DMF, 1 h, 2.) DMF, 1 h;

DOI:10.1021/jm9704309

upstream raw materials:

1-Iodoheptane

(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-3-nitro-2-naphthyl)phenylamine

bromobenzene

5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-3-nitro-2-naphthylamine

Downstream raw materials:

N-[3-(Heptyl-phenyl-amino)-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl]-terephthalamic acid methyl ester

N-Heptyl-5,5,8,8-tetramethyl-N-phenyl-5H,6H,7H,8H-naphthalene-2,3-diamine

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