.beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl-

Base Information

Chemical Name:.beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl-
CAS No.:72358-27-1
Molecular Formula:C20H38 N2 O11
Molecular Weight:482.53
Hs Code.:

Synonyms:.beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl-

Suppliers and Price of .beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of .beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl-

Chemical Property:

PSA：213.42000
LogP:-2.61880

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of .beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl-

There total 12 articles about .beta.-D-Glucopyranoside, 6-aminohexyl 2-(acetylamino)-2-deoxy-4-O-.beta.-D-galactopyranosyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 74666-20-9
6-<(Benzyloxycarbonyl)amino>hexyl O-(β-D-galactopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 72358-27-1
6-Aminohexyl O-(β-D-galactopyranosyl)-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; water; for 4h;
DOI:10.1002/jlac.199619961111

Reference yield:

: 209671-46-5
6-azidohexyl (β-D-galactopyranosyl)-(1→4)-2-acetamido-2-deoxy-β-D-glucopyranoside

: 72358-27-1
6-Aminohexyl O-(β-D-galactopyranosyl)-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With formic acid; palladium; In methanol; at 20 ℃; for 16h;
DOI:10.1016/S0040-4020(98)00294-4

Reference yield:

: 129647-37-6
O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-1,3,6-tri-O-acetyl-2-deoxy-2-phthalimido-α,β-D-glucopyranose

: 72358-27-1
6-Aminohexyl O-(β-D-galactopyranosyl)-(1->4)-2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 7.90 g / molecular sieves 4 Angstroem; trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 3 h / 0 - 20 °C

2: NaOMe / methanol / 1.5 h / 20 °C

3: hydrazine hydrate / methanol / 4 h / Heating

4: 3.79 g / methanol; ethanol / 5.7 h / 0 °C

5: 2.02 g / HCO₂H / Pd-black / methanol / 16 h / 20 °C

With formic acid; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium methylate; hydrazine hydrate; palladium; In methanol; ethanol; 1,2-dichloro-ethane; 1: glycosylation / 2: Deacetylation / 3: deprotection / 4: Acetylation / 5: Catalytic hydrogenation;
DOI:10.1016/S0040-4020(98)00294-4