Technology Process of C24H36SO3
There total 9 articles about C24H36SO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
at 20 ℃;
for 16h;
DOI:10.1021/ol990114j
- Guidance literature:
-
Multi-step reaction with 6 steps
1: quinoline / Lindlar catalyst / hexane / -10 °C
2: tetrahydrofuran / 0.33 h / 20 °C
3: LiBr / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / Heating
4: 81 percent / dimethylformamide / 4 h / 110 °C
5: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C
6: 84 percent / p-TsOH / methanol / 16 h / 20 °C
With
quinoline; toluene-4-sulfonic acid; lithium bromide; lithium diisopropyl amide;
Lindlar's catalyst;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ol990114j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 82 percent / NaI / acetone / 48 h / Heating
2: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C
3: 84 percent / p-TsOH / methanol / 16 h / 20 °C
With
toluene-4-sulfonic acid; sodium iodide; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; acetone;
DOI:10.1021/ol990114j