1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride

Base Information

Chemical Name:1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride
CAS No.:72335-83-2
Molecular Formula:C10H15 Cl O
Molecular Weight:186.6785
Hs Code.:
DSSTox Substance ID:DTXSID30505730
Wikidata:Q82361022
Mol file:72335-83-2.mol

Synonyms:72335-83-2;1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride;SCHEMBL10824184;DTXSID30505730

Suppliers and Price of 1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride

Chemical Property:

PSA：17.07000
LogP:3.27840
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:186.0811428
Heavy Atom Count:12
Complexity:180

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC1(CCCCC1)C(=O)Cl

Technology Process of 1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride

There total 4 articles about 1-(Prop-2-en-1-yl)cyclohexane-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72335-50-3
1-(1-prop-2-enyl)cyclohexanecarboxylic acid

: 72335-83-2
1-allylcyclohexane-1-carboxylic acid chloride

Guidance literature:: With thionyl chloride; at 25 ℃; for 1h;
DOI:10.1021/jo00321a017

Reference yield:

: 4630-82-4
methyl cyclohexylcarboxylate

: 72335-83-2
1-allylcyclohexane-1-carboxylic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / iPr₂NLi / tetrahydrofuran / 2 h / -78 °C

2: 92 percent / 15percent ethanolic KOH / 48 h / Heating

3: sodium, oxalyl chloride / diethyl ether / 3 h / Heating

With potassium hydroxide; oxalyl dichloride; sodium; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)96036-3

Reference yield:

: 67838-02-2
methyl 1-allylcyclohexane-1-carboxylate

: 72335-83-2
1-allylcyclohexane-1-carboxylic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 15percent ethanolic KOH / 48 h / Heating

2: sodium, oxalyl chloride / diethyl ether / 3 h / Heating

With potassium hydroxide; oxalyl dichloride; sodium; In diethyl ether;
DOI:10.1016/S0040-4020(01)96036-3