(R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate

Base Information

Chemical Name:(R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate
CAS No.:1415547-13-5
Molecular Formula:C₂₆H₄₁NO₅
Molecular Weight:447.615
Hs Code.:

Synonyms:(R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate

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Chemical Property of (R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate

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Technology Process of (R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate

There total 1 articles about (R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7766-50-9
1-undecen-11-ylbromide

: 76757-90-9
N-(tert-butoxycarbonyl)-D-tyrosine methyl ester

: 1415547-13-5
(R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate

Guidance literature:: With potassium carbonate; In acetonitrile; for 18h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2012.10.069

Reference yield:

: 1415547-13-5
(R)-methyl 2-(tert-butoxycarbonylamino)-3-(4-(undec-10-enyloxy)phenyl)propanoate

: 1415547-06-6
N₁-((S)-1-(4-(hex-5-enyloxy)phenyl)-2-hydroxyethyl)-N₃-((R)-1-hydroxy-3-(4-(undec-10-enyloxy)phenyl)propan-2-yl)-2,2-dimethylmalonamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / tetrahydrofuran; water / 18 h / Inert atmosphere; Reflux

3: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane; N,N-dimethyl-formamide / 93 h / 20 °C / Inert atmosphere

With lithium borohydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.10.069