4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine

Base Information

• Chemical Name: 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine
• CAS No.: 1380109-36-3
• Molecular Formula: C₇₈H₈₆N₄O₄S₂
• Molecular Weight: 1207.7

Synonyms:4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine

Chemical Property of 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine

Chemical Property:

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Technology Process of 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine

There total 2 articles about 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4,4'-dibromo-2,2'-bipyridine (18511-71-2) + N-(4-(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine → 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine (1380109-36-3)

Guidance literature:

With water; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 40h; Reflux;

Reference yield:

4,4'-dibromo-2,2'-bipyridine (18511-71-2) + N-(4-(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine (1380109-35-2) → 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine (1380109-36-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 40h; Reflux;

DOI:10.1039/c2cc00136e

Reference yield: 52.5%

4,4'-diethoxy-2,2'-bipyridine (53094-09-0) + [Ru(2-(2,4-bis(trifluoromethyl)phenyl)pyridine)(acetonitrile)4](PF6) (1360715-03-2) + 4,4'-di(N-(4-(5-thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine)-2,2'-bipyridine (1380109-36-3) → Ru(C5H4NC6H2(CF3)2)(C5H3(COOC2H5)NC5H3(COOC2H5)N)((C5H3((C6H13OC6H4)2NC6H4C4H2S)N)2)(1+)*PF6(1-)=[RuC107H108F6N7O8S2]PF6 (1380595-37-8)

Guidance literature:

In ethanol; chloroform; for 1.5h; Reflux;

upstream raw materials:

4,4'-dibromo-2,2'-bipyridine

N-(4-(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophen-2-yl)phenyl)-4-(hexyloxy)-N-(4-(hexyloxy)phenyl)benzenamine

Downstream raw materials:

Ru(C₅H₄NC₆H₂(CF₃)2)(C₅H₃(COOC₂H₅)NC₅H₃(COOC₂H₅)N)((C₅H₃((C₆H₁₃OC₆H₄)2NC₆H₄C₄H₂S)N)2)⁽¹⁺⁾*PF₆^(1-)=[RuC₁₀₇H₁₀₈F₆N₇O₈S₂]PF₆

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