hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

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Chemical Name:hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide
CAS No.:928211-48-7
Molecular Formula:C₂₅H₄₄N₄O₉S
Molecular Weight:576.712
Hs Code.:

Synonyms:hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

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Chemical Property of hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

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Technology Process of hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

There total 6 articles about hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 3,6,9,12,15-pentaoxaheptadecane-1,17-diamine dihydrochloride

: 142319-48-0
5-(4-Sulfamoyl-benzylcarbamoyl)-pentanoic acid

: 928211-48-7
hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 23 ℃;
DOI:10.1021/ja066780e

Reference yield:

: 109789-40-4
3,6,9,12,15-pentaoxaheptadecane-1,17-diyl dimethanesulfonate

: 928211-48-7
hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / dimethylformamide / 16 h / 50 °C

2: H₂; HCl / Pd/C / ethanol

3: 40 percent / 1-ethyl-3-[3-dimethylaminopropyl]carbodiimide hydrochloride; DIEA / dimethylformamide / 23 °C

With hydrogenchloride; sodium azide; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja066780e

Reference yield:

: 356046-26-9,82055-94-5
1-azido-2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethane

: 928211-48-7
hexanedioic acid {2-[2-(2-{2-[2-(2-amino-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-amide 4-sulfamoyl-benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂; HCl / Pd/C / ethanol

2: 40 percent / 1-ethyl-3-[3-dimethylaminopropyl]carbodiimide hydrochloride; DIEA / dimethylformamide / 23 °C

With hydrogenchloride; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja066780e