1-(1-cyclohexene)-ethyl-2,4-pentadienoate

Base Information

Chemical Name:1-(1-cyclohexene)-ethyl-2,4-pentadienoate
CAS No.:97329-95-8
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:1-(1-cyclohexene)-ethyl-2,4-pentadienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1-cyclohexene)-ethyl-2,4-pentadienoate

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Technology Process of 1-(1-cyclohexene)-ethyl-2,4-pentadienoate

There total 1 articles about 1-(1-cyclohexene)-ethyl-2,4-pentadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102651-85-4
(E)-3-(cyclohex-1-en-1-yl)acrylaldehyde

: 188945-44-0
ethyl 2-[bis(2-isopropylphenoxy)phosphoryl]acetate

: 1423124-54-2
(2Z,4E)-ethyl 5-(cyclohex-1-en-1-yl)penta-2,4-dienoate

: 97329-95-8
1-(1-cyclohexene)-ethyl-2,4-pentadienoate

Guidance literature:: ethyl 2-[bis(2-isopropylphenoxy)phosphoryl]acetate; With N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; methanol; at -78 ℃; for 0.25h; Inert atmosphere;

(E)-3-(cyclohex-1-en-1-yl)acrylaldehyde; In tetrahydrofuran; methanol; for 10h; Overall yield = 60 %; Inert atmosphere;
DOI:10.1016/j.phytochem.2012.08.001

Reference yield: 64.0%

: 97329-95-8
1-(1-cyclohexene)-ethyl-2,4-pentadienoate

: 145299-81-6
1-(1-cyclohexene)-2,4-pentadien-5-ol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; at -70 ℃; for 5h;
DOI:10.1016/0022-2860(92)80123-Y

Reference yield:

: 97329-95-8
1-(1-cyclohexene)-ethyl-2,4-pentadienoate

: 114438-43-6
pentademethylretinal

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / (i-Bu)2AlH / diethyl ether / 5 h / -70 °C

2: 64 percent / MnO₂ / CH₂Cl₂ / 6 h / Ambient temperature

3: 1.) NaH / 1.) THF, 0 deg C, 2.) THF, 0 deg C, 30 min

4: 55 percent / (i-Bu)2AlH / diethyl ether / 5 h / -70 °C

5: 62 percent / MnO₂ / CH₂Cl₂ / 6 h / Ambient temperature

With manganese(IV) oxide; sodium hydride; diisobutylaluminium hydride; In diethyl ether; dichloromethane;
DOI:10.1016/0022-2860(92)80123-Y