Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester
CAS No.:147410-05-7
Molecular Formula:C₁₉H₂₀O₆S
Molecular Weight:376.43
Hs Code.:

Synonyms:Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

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Chemical Property of Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

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Technology Process of Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

There total 4 articles about Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147410-01-3
(S)-5-Benzyloxymethyl-3-tosyloxy-2(5H)-furanone

: 147410-05-7
Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h; under 1520 Torr; Ambient temperature;
DOI:10.1016/S0040-4020(01)85821-X

Reference yield:

: 78508-91-5
5-benzyloxy-2-hydroxy-3-hydroxy-D-ribonolactone

: 147410-05-7
Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / pyridine / 1) 0 deg C, 2 h, 2) r.t., 24 h

2: 239 mg / H₂ / 10percent Pd/C / ethyl acetate / 16 h / 1520 Torr / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0040-4020(01)85821-X

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 147410-05-7
Toluene-4-sulfonic acid (3S,5S)-5-benzyloxymethyl-2-oxo-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / pyridine / 1) 0 deg C, 2 h, 2) r.t., 24 h

2: 239 mg / H₂ / 10percent Pd/C / ethyl acetate / 16 h / 1520 Torr / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0040-4020(01)85821-X